TA Instruments

AR1756-0017f

15/03/2013 15:21:44

Sample name	ASW Blank coupon#20 + DI + beads 300rad/s
Sample notes	 
Experiment notes	DI Deionised water, 25 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1756
Run number	17 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 15:21:44

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	No
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	No

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	0.4094 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	2
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.14 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

0.99600	299.9	-701.58	10000	20.0	0.4117	0.996	-228.7	374.9	-0.6100	1677	242.7650	0.01194	303.46	30346	3.411E-3	0.0	0.0
1.9960	300.0	662.55	10000	20.0	0.3928	1.996	216.0	375.0	0.5759	1600	494.0150	0.01138	617.52	61752	3.411E-3	0.0	0.0
3.0120	300.0	668.57	10000	20.0	0.3900	3.012	217.9	375.0	0.5811	1589	870.8780	0.01130	1088.6	1.0886E5	3.411E-3	0.1	0.1
4.0000	300.0	665.39	10000	20.0	0.3893	4.000	216.9	375.0	0.5784	1586	1124.1200	0.01128	1405.2	1.4052E5	3.411E-3	0.1	0.1
5.0000	300.0	651.76	10000	20.0	0.3928	5.000	212.4	375.0	0.5665	1600	1373.5300	0.01138	1716.9	1.7169E5	3.411E-3	0.1	0.1
5.9960	300.0	659.24	10000	20.0	0.3889	5.996	214.9	375.0	0.5730	1585	1752.8700	0.01127	2191.1	2.1911E5	3.411E-3	0.1	0.1
6.9960	300.0	646.11	10000	20.0	0.3887	6.996	210.6	375.0	0.5616	1584	2001.8900	0.01126	2502.4	2.5024E5	3.411E-3	0.1	0.1
8.0000	300.0	642.61	10000	20.0	0.3904	8.000	209.5	375.0	0.5586	1590	2378.8301	0.01131	2973.5	2.9735E5	3.411E-3	0.1	0.1
9.0120	300.0	646.34	10000	20.0	0.3893	9.012	210.7	375.0	0.5618	1586	2630.0901	0.01128	3287.6	3.2876E5	3.411E-3	0.2	0.2
9.9960	300.0	645.16	10000	20.0	0.3944	9.996	210.3	375.0	0.5607	1607	2881.7300	0.01143	3602.2	3.6022E5	3.411E-3	0.2	0.2
10.996	300.0	652.51	10000	20.0	0.3855	10.996	212.7	375.0	0.5672	1571	3258.5400	0.01117	4073.2	4.0732E5	3.411E-3	0.2	0.2
12.000	300.0	643.80	10000	20.0	0.3893	12.000	209.8	375.0	0.5595	1586	3509.8201	0.01128	4387.3	4.3873E5	3.411E-3	0.2	0.2
12.996	300.0	631.34	10000	20.0	0.3985	12.996	205.8	375.0	0.5487	1624	3886.8899	0.01154	4858.6	4.8586E5	3.411E-3	0.2	0.2
14.000	300.0	634.87	10000	20.0	0.3855	14.000	206.9	375.0	0.5518	1571	4144.3701	0.01117	5180.5	5.1805E5	3.411E-3	0.2	0.2
14.996	300.0	639.72	10000	20.0	0.3875	14.996	208.5	375.0	0.5560	1579	4389.4302	0.01123	5486.8	5.4868E5	3.411E-3	0.2	0.2
15.996	300.0	637.33	10000	20.0	0.3924	15.996	207.7	375.0	0.5540	1599	4766.6099	0.01137	5958.3	5.9583E5	3.411E-3	0.3	0.3
16.996	300.0	637.88	10000	20.0	0.3960	16.996	207.9	375.0	0.5545	1614	5017.8901	0.01148	6272.4	6.2724E5	3.411E-3	0.3	0.3
17.996	300.0	646.70	10000	20.0	0.3971	17.996	210.8	375.0	0.5621	1618	5396.6201	0.01151	6745.8	6.7458E5	3.411E-3	0.3	0.3
19.000	300.0	645.11	10000	20.0	0.3835	19.000	210.3	375.0	0.5607	1562	5646.0801	0.01111	7057.6	7.0576E5	3.411E-3	0.3	0.3
19.996	300.0	639.41	10000	20.0	0.3902	19.996	208.4	375.0	0.5557	1590	5897.3398	0.01130	7371.7	7.3717E5	3.411E-3	0.3	0.3
20.996	300.0	641.97	10000	20.0	0.3833	20.996	209.3	375.0	0.5580	1562	6276.5601	0.01110	7845.7	7.8457E5	3.411E-3	0.3	0.3
21.992	300.0	643.89	10000	20.0	0.3869	21.992	209.9	375.0	0.5597	1576	6525.7100	0.01121	8157.1	8.1571E5	3.411E-3	0.4	0.4
22.996	300.0	628.42	10000	20.0	0.3914	22.996	204.8	375.0	0.5462	1595	6777.0400	0.01134	8471.3	8.4713E5	3.411E-3	0.4	0.4
24.000	300.0	628.49	10000	20.0	0.3869	24.000	204.9	375.0	0.5463	1576	7154.4702	0.01121	8943.1	8.9431E5	3.411E-3	0.4	0.4
24.996	300.0	632.59	10000	20.0	0.3900	24.996	206.2	375.0	0.5498	1589	7405.4399	0.01130	9256.8	9.2568E5	3.411E-3	0.4	0.4
25.996	300.0	642.28	10000	20.0	0.3930	25.996	209.4	375.0	0.5583	1601	7782.3501	0.01139	9727.9	9.7279E5	3.411E-3	0.4	0.4
26.996	300.0	642.89	10000	20.0	0.3898	26.996	209.5	375.0	0.5588	1588	8033.7202	0.01129	10042	1.0042E6	3.411E-3	0.4	0.4
27.996	300.0	636.31	10000	20.0	0.3952	27.996	207.4	375.0	0.5531	1610	8286.1602	0.01145	10358	1.0358E6	3.411E-3	0.5	0.5
29.000	300.0	628.77	10000	20.0	0.3908	29.000	204.9	375.0	0.5465	1592	8663.6904	0.01132	10830	1.0830E6	3.411E-3	0.5	0.5
29.996	300.0	629.22	10000	20.0	0.3950	29.996	205.1	375.0	0.5469	1609	8913.5000	0.01145	11142	1.1142E6	3.411E-3	0.5	0.5
30.996	300.0	634.30	10000	20.0	0.3924	30.996	206.8	375.0	0.5513	1599	9297.5801	0.01137	11622	1.1622E6	3.411E-3	0.5	0.5
31.992	300.0	649.48	10000	20.0	0.3861	31.992	211.7	375.0	0.5646	1573	9541.5801	0.01119	11927	1.1927E6	3.411E-3	0.5	0.5
32.996	300.0	640.95	10000	20.0	0.3922	32.996	208.9	375.0	0.5571	1598	9795.4902	0.01136	12244	1.2244E6	3.411E-3	0.5	0.5
34.000	300.0	644.06	10000	20.0	0.3812	34.000	209.9	375.0	0.5598	1553	10171.000	0.01105	12714	1.2714E6	3.411E-3	0.6	0.6
34.996	300.0	634.40	10000	20.0	0.3839	34.996	206.8	375.0	0.5514	1564	10421.900	0.01112	13027	1.3027E6	3.411E-3	0.6	0.6
36.008	300.0	651.51	10000	20.0	0.3879	36.008	212.4	375.0	0.5663	1581	10800.900	0.01124	13501	1.3501E6	3.411E-3	0.6	0.6
36.996	300.0	655.92	10000	20.0	0.3794	36.996	213.8	375.0	0.5701	1546	11052.100	0.01099	13815	1.3815E6	3.411E-3	0.6	0.6
37.996	300.0	635.09	10000	20.0	0.3922	37.996	207.0	375.0	0.5520	1598	11301.000	0.01136	14126	1.4126E6	3.411E-3	0.6	0.6
39.000	300.0	623.85	10000	20.0	0.3808	39.000	203.3	375.0	0.5422	1552	11677.900	0.01103	14597	1.4597E6	3.411E-3	0.7	0.7
39.996	300.0	645.35	10000	20.0	0.3920	39.996	210.4	375.0	0.5609	1597	11929.300	0.01136	14912	1.4912E6	3.411E-3	0.7	0.7
41.056	300.0	633.77	10000	20.0	0.3930	41.056	206.6	375.0	0.5509	1601	12306.300	0.01139	15383	1.5383E6	3.411E-3	0.7	0.7
41.992	300.0	647.18	10000	20.0	0.3841	41.992	210.9	375.0	0.5626	1565	12557.700	0.01113	15697	1.5697E6	3.411E-3	0.7	0.7
42.996	300.0	639.70	10000	20.0	0.3954	42.996	208.5	375.0	0.5561	1611	12809.200	0.01146	16012	1.6012E6	3.411E-3	0.7	0.7
43.992	300.0	637.62	10000	20.0	0.3865	43.992	207.8	375.0	0.5542	1575	13185.900	0.01120	16482	1.6482E6	3.411E-3	0.7	0.7
44.992	300.0	640.09	10000	20.0	0.3812	44.992	208.6	375.0	0.5563	1553	13437.500	0.01104	16797	1.6797E6	3.411E-3	0.7	0.7
45.996	300.0	639.51	10000	20.0	0.3898	45.996	208.4	375.0	0.5559	1588	13688.500	0.01129	17111	1.7111E6	3.411E-3	0.8	0.8
46.996	300.0	651.60	10000	20.0	0.3936	46.996	212.4	375.0	0.5664	1604	14065.700	0.01140	17582	1.7582E6	3.411E-3	0.8	0.8
47.996	300.0	634.10	10000	20.0	0.3881	47.996	206.7	375.0	0.5512	1581	14316.900	0.01125	17896	1.7896E6	3.411E-3	0.8	0.8
49.000	300.0	633.79	10000	20.0	0.3881	49.000	206.6	375.0	0.5509	1581	14695.200	0.01125	18369	1.8369E6	3.411E-3	0.8	0.8
49.996	300.0	653.24	10000	20.0	0.3877	49.996	212.9	375.0	0.5678	1580	14945.100	0.01123	18681	1.8681E6	3.411E-3	0.8	0.8
50.996	300.0	641.06	10000	20.0	0.3855	50.996	209.0	375.0	0.5572	1571	15197.300	0.01117	18997	1.8997E6	3.411E-3	0.8	0.8
51.992	300.0	634.69	10000	20.0	0.3893	51.992	206.9	375.0	0.5516	1586	15574.900	0.01128	19469	1.9469E6	3.411E-3	0.9	0.9
53.040	300.0	633.24	10000	20.0	0.3920	53.040	206.4	375.0	0.5504	1597	15824.800	0.01136	19781	1.9781E6	3.411E-3	0.9	0.9
54.000	300.0	630.60	10000	20.0	0.3851	54.000	205.5	375.0	0.5480	1569	16079.300	0.01115	20099	2.0099E6	3.411E-3	0.9	0.9
54.996	300.0	639.71	10000	20.0	0.3810	54.996	208.5	375.0	0.5560	1552	16453.199	0.01104	20567	2.0567E6	3.411E-3	0.9	0.9
55.992	300.0	640.29	10000	20.0	0.3902	55.992	208.7	375.0	0.5566	1590	16705.900	0.01131	20882	2.0882E6	3.411E-3	0.9	0.9
57.004	300.0	635.55	10000	20.0	0.3853	57.004	207.2	375.0	0.5524	1570	17082.699	0.01116	21353	2.1353E6	3.411E-3	1.0	1.0
57.992	300.0	632.70	10000	20.0	0.3812	57.992	206.2	375.0	0.5499	1553	17335.400	0.01105	21669	2.1669E6	3.411E-3	1.0	1.0
59.000	300.0	633.00	10000	20.0	0.3849	59.000	206.3	375.0	0.5502	1568	17584.301	0.01115	21980	2.1980E6	3.411E-3	1.0	1.0
60.012	300.0	642.63	10000	20.0	0.3881	60.012	209.5	375.0	0.5586	1581	17961.100	0.01124	22451	2.2451E6	3.411E-3	1.0	1.0

